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Beilstein J. Org. Chem. 2016, 12, 2046–2054, doi:10.3762/bjoc.12.193
Graphical Abstract
Scheme 1: Synthesis of menthol.
Scheme 2: Synthesis of para-menthane-3,8-diol.
Scheme 3: Synthesis of para-menthane diester derivatives.
Figure 1: PMD conversion using stoichiometric quantities of acetic anhydride.
Figure 2: Product distribution as a function of time.
Figure 3: Product distribution as a function of time.
Figure 4: Effect of molar ratio in product distribution.
Scheme 4: Synthesis of para-menthane mono-ester derivatives.